反应条件
1: allyl(p-methoxybenzyl)ether With pyridinium tribromide in dichloromethane T=20°C; Inert atmosphere; 2: With 1,8-diazabicyclo[5.4.0]undec-7-ene in dichloromethane T=0 - 60°C; Inert atmosphere; 3: dimethyl zinc With PEPPSI™-IPr in tetrahydrofuran; hexane; dichloromethane T=0 - 60°C; Negishi Coupling; 2 h; Inert atmosphere;
参考文献
Kutsumura, Noriki; Matsubara, Yusuke; Niwa, Kentaro; Ito, Ai; Saito, Takao
European Journal of Organic Chemistry, 2013 , # 16 p. 3337 - 3346