反应条件
1.1: dimethyl sulfoxide; oxalyl dichloride / dichloromethane / 0.5 h / -78 °C 1.2: 0.5 h / -78 °C 2.1: tetrahydrofuran / 16 h / 0 - 20 °C / |Inert atmosphere 3.1: iodine / water; 1,4-dioxane / 16 h / 20 °C View Scheme
参考文献
Davies, Stephen G.; Figuccia, Aude L. A.; Fletcher, Ai M.; Roberts, Paul M.; Thomson, James E.
Organic Letters, 2013 , vol. 15, # 8 p. 2042 - 2045