1.1: lithium diisopropylamide; HMPA / tetrahydrofuran / -20 °C 1.2: oxygen / tetrahydrofuran / -78 °C 2.1: aq. HCl / 50 °C View Scheme
参考文献
Mukherjee, Arnab; Angeles-Boza, Alfredo M.; Huff, Gregory S.; Roth, Justine P.
Journal of the American Chemical Society, 2011 , vol. 133, # 2 p. 227 - 238
in ethanol prepn. by refluxing ZnO with excess of carboxylic acid in EtOH for about2 h; cooled; ppt. filtered off; washed (EtOH) repeatedly; collected; kept over silica gel in vac. desiccator; elem. anal.;
参考文献
Taylor, Richard A.; Ellis, Henry A.
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 2007 , vol. 68, # 1 p. 99 - 107