反应条件
1: 4-(N,N-dimethlyamino)pyridine; dicyclohexyl-carbodiimide / dichloromethane / 16 h / -20 - 4 °C / Inert atmosphere
2: sodium tetrahydroborate; acetic acid / 4 °C / Inert atmosphere
3: methanol / Reflux; Inert atmosphere
4: palladium 10 on activated carbon; hydrogen / ethyl acetate / 16 h / 760.05 Torr
View Scheme
参考文献
Morgenroth, Agnieszka; Urusova, Elizaveta A.; Dinger, Cornelia; Al-Momani, Ehab; Kull, Thomas; Glatting, Gerhard; Frauendorf, Holm; Jahn, Olaf; Mottaghy, Felix M.; Reske, Sven N.; Zlatopolskiy, Boris D.
Chemistry - A European Journal, 2011 , vol. 17, # 36 p. 10144 - 10150