反应条件
1: oxalyl dichloride; N,N-dimethyl-formamide
2: 4-(N,N-dimethlyamino)pyridine; trichloromonobromomethane; Fonderma / 4 h / Reflux
3: N,N-dimethyl-formamide / 2 h / Reflux
4: hydrogenchloride / water / 12 h / Reflux
View Scheme
参考文献
Ho, Jonathan Z.; Wallace, Michael A.; Tang, Yui S.; Zhang, Andy S.; Braun, Matthew P.
Journal of Labelled Compounds and Radiopharmaceuticals, 2010 , vol. 53, # 5-6 p. 251 - 253