反应条件
1: 85 percent / pyridinium chlorochromate / CH2Cl2 / 1 h 2: 87.5 percent / p-toluenesulfonic acid / benzene / 20 h / Heating 3: 1.) 9-BBN / 1.) THF, 25 deg C, 3 h, 2.) methanol, reflux, 2 h 4: 1.) 9-BBN, 2.) lithium diisopropylamide, 3.) NaOH, H2O2 5: diethyl ether 6: 70 percent / LAH / diethyl ether / 5 h View Scheme
参考文献
Dhillon, Ranjit S.; Singh, Rupinder P.; Singh, Jasvinder
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1995 , vol. 34, # 8 p. 718 - 721
