iodine in tetrachloromethane Kinetics; byproducts: CH3I, C2H5I; Hg-compound added to a soln. of iodine at 25°C in the dark; not isolated, monitored by UV;
参考文献
Journal of the American Chemical Society, , vol. 102, # 7 p. 2141 - 2152
Journal of the Chemical Society [Section] A: Inorganic, Physical, Theoretical, , p. 2566 - 2569
Journal of Organometallic Chemistry, , vol. 32, p. 323 - 330
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反应条件
potassium iodide in tetrahydrofuran byproducts: Hg2Cl2; heating of Zr-compd. and HgCl2 (80°C, 4 h), solvent removal (vac.), distn. with water vapour into aq. KI (pptn.); filtration, drying;
参考文献
Inorganica Chimica Acta, , vol. 44, p. L285 - L288