反应条件
in hydrogenchloride P8W48 compd. and LiCl dissolved in 0.1 M HCl, NaBPh4 added to remove K cations, then Mo compd. added, stirring at room temp. (6 h), NaCl added, 12 h at 4-6°C; ppt. filtered, washed (H2O, EtOH, ether), dried (air); elem. anal., EDX;
参考文献
Korenev, Vladimir S.; Floquet, Sebastien; Marrot, Jerome; Haouas, Mohamed; Mbomekalle, Israel-Martyr; Taulelle, Francis; Sokolov, Maxim N.; Fedin, Vladimir P.; Cadot, Emmanuel
Inorganic Chemistry, 2012 , vol. 51, # 4 p. 2349 - 2358
