Boc-D-3,3-二苯基丙氨酸合成路线 （共 15 条）
反应条件
1.1: H2 / 20 percent Pd(OH)2/C / formic acid / 6 h / 20 °C / 5171.48 Torr 1.2: 78 percent / 1M aq. NaOH / ethyl acetate / 4 h 2.1: 88 percent / Jones reagent / acetone / 4 h / 0 °C View Scheme
参考文献
Heterocycles, , vol. 57, # 6 p. 1143 - 1148
反应条件
1.1: 96 percent / KOH / ethanol / 2 h / 20 °C 2.1: H2 / 20 percent Pd(OH)2/C / formic acid / 6 h / 20 °C / 5171.48 Torr 2.2: 78 percent / 1M aq. NaOH / ethyl acetate / 4 h 3.1: 88 percent / Jones reagent / acetone / 4 h / 0 °C View Scheme
参考文献
Heterocycles, , vol. 57, # 6 p. 1143 - 1148
反应条件
1: 95 percent / TEA / tetrahydrofuran 2: 88 percent / Cs2CO3 / methanol 3: 80 percent / Jones reagent View Scheme
参考文献
Tetrahedron Letters, , vol. 36, # 49 p. 8961 - 8964
反应条件
1: 79 percent / Na / NH3 / 0.25 h 2: 95 percent / TEA / tetrahydrofuran 3: 88 percent / Cs2CO3 / methanol 4: 80 percent / Jones reagent View Scheme
参考文献
Tetrahedron Letters, , vol. 36, # 49 p. 8961 - 8964
反应条件
1: 88 percent / Cs2CO3 / methanol 2: 80 percent / Jones reagent View Scheme
参考文献
Tetrahedron Letters, , vol. 36, # 49 p. 8961 - 8964
