反应条件
1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct; potassium acetate / 1,4-dioxane / 3 h / 100 °C / |Inert atmosphere
2: [RhCl(η2:η2-cycloocta-1,5-diene)]2; bis(η3-allyl-μ-chloropalladium(II)); 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl; potassium phosphate / 1,1-dimethylpropan-1-ol; methanol / 16.08 h / 20 - 110 °C / |Inert atmosphere; |Sealed tube
View Scheme
参考文献
Zhang, Lei; Sonaglia, Lorenzo; Stacey, Jason; Lautens, Mark
Organic Letters, 2013 , vol. 15, # 9 p. 2128 - 2131