3,4-二氢-2-萘基三氟甲烷磺酸酯合成路线 （共 19 条）
反应条件
in dichloromethane T=20°C; 24 h;
参考文献
Herrera, Antonio; Martinez-Alvarez, Roberto; Chioua, Mourad; Chatt, Rachid; Chioua, Rachid; Sanchez, Angel; Almy, John
Tetrahedron, 2006 , vol. 62, # 12 p. 2799 - 2811
反应条件
in dichloromethane T=20°C; 24 h;
参考文献
Herrera, Antonio; Martinez-Alvarez, Roberto; Chioua, Mourad; Chatt, Rachid; Chioua, Rachid; Sanchez, Angel; Almy, John
Tetrahedron, 2006 , vol. 62, # 12 p. 2799 - 2811
反应条件
pyridine in dichloromethane T=25°C; 5 h; Inert atmosphere;
参考文献
Wu, Xiaojin; Lu, Yunpeng; Hirao, Hajime; Zhou, Jianrong
Chemistry - A European Journal, 2013 , vol. 19, # 19 p. 6014 - 6020
反应条件
2,6-di-tert-butyl-4-methylpyridine Yield given. Title compound not separated from byproducts;
参考文献
Kamekawa, Hisato; Senboku, Hisanori; Tokuda, Masao
Tetrahedron Letters, 1998 , vol. 39, # 12 p. 1591 - 1594
反应条件
1: ethylmagnesium bromide; triethylsilylethynylmagnesium bromide in tetrahydrofuran T=20°C; 0.5 h; 2: trifluoromethanesulfonic acid 3,4-dihydronaphthalen-2-yl ester With Co(acetylacetonate)3 in tetrahydrofuran T=20°C; 2 h; Further stages.;
参考文献
Shirakawa, Eiji; Sato, Takahiro; Imazaki, Yusuke; Kimura, Takahiro; Hayashi, Tamio
Chemical Communications, 2007 , # 43 p. 4513 - 4515
反应条件
triphenylphosphine; Co(acetylacetonate)3 in tetrahydrofuran
T=20°C; 3 h;
参考文献
Shirakawa, Eiji; Imazaki, Yusuke; Hayashi, Tamio
Chemistry Letters, 2008 , vol. 37, # 6 p. 654 - 655
反应条件
1-methyl-pyrrolidin-2-one; iron (III) acetylacetonate in tetrahydrofuran
T=-30°C;
参考文献
Scheiper, Bodo; Bonnekessel, Melanie; Krause, Helga; Fuerstner, Alois
Journal of Organic Chemistry, 2004 , vol. 69, # 11 p. 3943 - 3949
反应条件
1-methyl-pyrrolidin-2-one; iron (III) acetylacetonate in tetrahydrofuran
T=-30°C;
参考文献
Scheiper, Bodo; Bonnekessel, Melanie; Krause, Helga; Fuerstner, Alois
Journal of Organic Chemistry, 2004 , vol. 69, # 11 p. 3943 - 3949
反应条件
[RuIII(2,4-pentanedionato)3]; 1,10-phenanthroline; ethylmagnesium bromide; lithium bromide in tetrahydrofuran
T=60°C; 24 h; Inert atmosphere;
参考文献
Shirakawa, Eiji; Imazaki, Yusuke; Hayashi, Tamio
Chemical Communications, 2009 , # 34 p. 5088 - 5090
