N-甲基-3-甲氧基苯胺合成路线 （共 31 条）
参考文献
Journal of the Chemical Society, , p. 3362,3370
反应条件
1: T=180°C; 0.75 h; 2: With sulfuric acid in water T=95°C; Knorr Quinoline synthesis; 0.75 h;
参考文献
Fonseca, Andrea S.C.; Soares, Ana M.S.; Goncalves, M. Sameiro T.; Costa, Susana P.G.
Tetrahedron, 2012 , vol. 68, # 38 p. 7892 - 7900
反应条件
hydrogenchloride; sodium nitrite
参考文献
Liu, Baoqing; Fan, Yang; Gao, Yang; Sun, Chao; Xu, Cheng; Zhu, Jin
Journal of the American Chemical Society, 2013 , vol. 135, # 1 p. 468 - 473
反应条件
1: sodium hydrogencarbonate / acetonitrile / 4 h / Inert atmosphere; Reflux 2: sodium tetrahydroborate; lithium bromide / tetrahydrofuran / 5 h / Reflux; Inert atmosphere View Scheme
参考文献
Otomo, Akira; Aoki, Isao; Miki, Hideki; Tazawa, Hidehisa; Yokoyama, Shiyoshi
Patent: US2012/172599 A1, 2012 ;
反应条件
potassium hydroxide in acetonitrile Inert atmosphereReflux;
参考文献
Hai, Yang; Chen, Juan-Juan; Zhao, Pei; Lv, Hongbin; Yu, Yi; Xu, Pingyong; Zhang, Jun-Long
Chemical Communications, 2011 , vol. 47, # 8 p. 2435 - 2437
参考文献
Stadlbauer, Wolfgang; Laschober, Rita; Kappe, Thomas
Liebigs Annalen der Chemie, 1990 , # 6 p. 531 - 539
反应条件
C27H36Cl2N2Zn; phenyl silane in tetrahydrofuran T=100°C; 20 h;
参考文献
Jacquet, Olivier; Frogneux, Xavier; Das Neves Gomes, Christophe; Cantat, Thibault
Chemical Science, 2013 , vol. 4, # 5 p. 2127 - 2131
反应条件
1.1: potassium hydroxide / acetonitrile / Inert atmosphere; Reflux
2.1: boron tribromide / dichloromethane / -78 - 20 °C / Inert atmosphere
2.2: Cooling with ice; Inert atmosphere
3.1: trichlorophosphate / 0.5 h / 0 °C / Inert atmosphere
3.2: 0 - 20 °C / Inert atmosphere
3.3: Inert atmosphere
View Scheme
参考文献
Hai, Yang; Chen, Juan-Juan; Zhao, Pei; Lv, Hongbin; Yu, Yi; Xu, Pingyong; Zhang, Jun-Long
Chemical Communications, 2011 , vol. 47, # 8 p. 2435 - 2437
反应条件
pyridine in diethyl ether
1.) -78 deg C, 1 min, 2.) RT;
参考文献
Andersen, Kenneth K.; Malver, Olaf
Journal of Organic Chemistry, 1983 , vol. 48, # 25 p. 4803 - 4807
反应条件
pyridine in diethyl ether
1.) -78 deg C, 1 min, 2.) RT;
参考文献
Andersen, Kenneth K.; Malver, Olaf
Journal of Organic Chemistry, 1983 , vol. 48, # 25 p. 4803 - 4807
