2,3-二氢-2-苯基-1H-1,3,2-二氮杂硼戊环并[4,5-b]吡啶合成路线 （共 6 条）
反应条件
in toluene byproducts: H2O; distg. the water with the solvent; filtering, recrystn. from toluene;
参考文献
Matteson,D.S.; Waldbillig,J.O.
Journal of Organic Chemistry, 1963 , vol. 28, p. 366 - 369
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Nyilas; Soloway
Journal of the American Chemical Society, 1959 , vol. 81, p. 2681
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Zimmer et al.
Naturwissenschaften, 1960 , vol. 47, p. 378
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Gmelin Handbook: B: B-Verb.1, 2.8.2.1.3, page 168 - 175
反应条件
in benzene byproducts: HCl; by heating at reflux for 8 h, cooling and filtering; recrystn. from benzene or vac. sublimation at 165°C 0.005-0.01 Torr;
参考文献
Pailer,M.; Fenzl,W.
Monatshefte fuer Chemie, 1961 , vol. 92, p. 1294 - 1299
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Dewar, M. J. S.; Kubba, V. P.; Pettit, R.
Journal of the Chemical Society, 1958 , p. 3073 - 3076
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Gmelin Handbook: B: B-Verb.1, 2.8.2.1.3, page 168 - 175
反应条件
1: diethyl ether View Scheme
参考文献
Gmelin Handbook: B: B-Verb.4, 3.6, page 66 - 88
反应条件
1: diethyl ether View Scheme
参考文献
Gmelin Handbook: B: B-Verb.4, 3.6, page 66 - 88
参考文献
Zimmer; Andrews; Sill
Arzneimittel-Forschung, 1967 , vol. 17, # 5 p. 607 - 609
参考文献
Gmelin Handbook: B: B-Verb.4, 3.6, page 66 - 88
