反应条件
Stage #1: <b>With</b> <a href="#" onclick="return RXDsubstances(event, this, '2036449', constants.ctx, '0')">phosphorus pentachloride</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '605264', constants.ctx, '0')">1,2-dichloro-ethane</a> <br />0.0833333 h; Reflux; <br />Stage #2: <b>With</b> <a href="#" onclick="return RXDsubstances(event, this, '11323438', constants.ctx, '0')">AlCl<sub>3</sub>, aluminium chloride</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '605264', constants.ctx, '0')">1,2-dichloro-ethane</a> <br /> Reflux; <br />Stage #3: <b>With</b> <a href="#" onclick="return RXDsubstances(event, this, '1098214', constants.ctx, '0')">hydrogenchloride</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '1209237', constants.ctx, '0')">ethylene glycol dimethyl ether</a>; <a href="#" onclick="return RXDsubstances(event, this, '3587155', constants.ctx, '0')">water</a> <br /> <br /> <br />
参考文献
Gu, Yan-Jing; Yan, Bing; Qiao, Xiao-Fei Journal of Solid State Chemistry, 2013 , vol. 199, p. 116 - 122