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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
143246-73-5
合成路线
（共 5 条）
143232-24-0
→
反应条件
143246-73-5
反应条件
Monoperoxyphthalic acid, magnesium salt in methanol T=0°C; 0.5 h;
参考文献
Williams; Ciccarone; MacTough; Rooney; Balani; Condra; Emini; Goldman; Greenlee; Kauffman; O'Brien; Sardana; Schleif; Theoharides; Anderson
Journal of Medicinal Chemistry, 1993 , vol. 36, # 9 p. 1291 - 1294
24621-70-3
1H-吲哚-2-甲醇
→
反应条件
143246-73-5
反应条件
1: 74 percent / n-Bu3P / tetrahydrofuran / 3 h / 20 °C 2: 55 percent / NaH / dimethylformamide / 6 h / 20 °C 3: 46 percent / monoperoxyphthalic acid magnesium salt (MMPP) / methanol / 0.5 h / 0 °C View Scheme
参考文献
Williams; Ciccarone; MacTough; Rooney; Balani; Condra; Emini; Goldman; Greenlee; Kauffman; O'Brien; Sardana; Schleif; Theoharides; Anderson
Journal of Medicinal Chemistry, 1993 , vol. 36, # 9 p. 1291 - 1294
1202-04-6
吲哚-2-羧酸甲酯
→
反应条件
143246-73-5
反应条件
1: 97 percent / LiAlH4 / tetrahydrofuran / 1 h / 0 °C 2: 74 percent / n-Bu3P / tetrahydrofuran / 3 h / 20 °C 3: 55 percent / NaH / dimethylformamide / 6 h / 20 °C 4: 46 percent / monoperoxyphthalic acid magnesium salt (MMPP) / methanol / 0.5 h / 0 °C View Scheme
参考文献
Williams; Ciccarone; MacTough; Rooney; Balani; Condra; Emini; Goldman; Greenlee; Kauffman; O'Brien; Sardana; Schleif; Theoharides; Anderson
Journal of Medicinal Chemistry, 1993 , vol. 36, # 9 p. 1291 - 1294
143232-23-9
→
反应条件
143246-73-5
反应条件
1: 55 percent / NaH / dimethylformamide / 6 h / 20 °C 2: 46 percent / monoperoxyphthalic acid magnesium salt (MMPP) / methanol / 0.5 h / 0 °C View Scheme
参考文献
Williams; Ciccarone; MacTough; Rooney; Balani; Condra; Emini; Goldman; Greenlee; Kauffman; O'Brien; Sardana; Schleif; Theoharides; Anderson
Journal of Medicinal Chemistry, 1993 , vol. 36, # 9 p. 1291 - 1294
882-33-7
二苯二硫醚
→
反应条件
143246-73-5
反应条件
1: 74 percent / n-Bu3P / tetrahydrofuran / 3 h / 20 °C 2: 55 percent / NaH / dimethylformamide / 6 h / 20 °C 3: 46 percent / monoperoxyphthalic acid magnesium salt (MMPP) / methanol / 0.5 h / 0 °C View Scheme
参考文献
Williams; Ciccarone; MacTough; Rooney; Balani; Condra; Emini; Goldman; Greenlee; Kauffman; O'Brien; Sardana; Schleif; Theoharides; Anderson
Journal of Medicinal Chemistry, 1993 , vol. 36, # 9 p. 1291 - 1294
