disodium hydrogenphosphate; sodium amalgam in tetrahydrofuran; methanol Inert atmosphere;

disodium hydrogenphosphate; sodium amalgam in tetrahydrofuran; methanol Inert atmosphere;

<b>Multi-step reaction with 3 steps<br /> </b>1: sodium azide / acetonitrile / 1 h / |Inert atmosphere<br />2: acetonitrile / 70 &deg;C / |Inert atmosphere<br />3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 0 &deg;C<br /> <br /> &nbsp;

<b>Multi-step reaction with 2 steps<br /> </b>1: acetonitrile / 70 &deg;C / |Inert atmosphere<br />2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 0 &deg;C<br /> <br /> &nbsp;