反应条件
1: LiAlH4 / diethyl ether / 15 h
2: ClSiMe3 / CH2Cl2 / 2 h / 20 °C
3: NEt3 / CH2Cl2 / 2 h
4: 1) Cl3COCO2CCl3, dimethylsulfoxide, 2) NEt3 / 1) CH2Cl2
5: 50 percent / tetrabutylammonium fluoride / tetrahydrofuran / 2 h / Ambient temperature
View Scheme
参考文献
Palomo, Claudio; Aizpurua, Jesus M.; Legido, Marta; Picard, Jean Paul; Dunogues, Jacques; Constantieux, Thierry
Tetrahedron Letters, 1992 , vol. 33, # 27 p. 3903 - 3906
