3-(4-氯苯基)-2-苯基吲哚合成路线 （共 11 条）
反应条件
potassium carbonate in acetonitrile T=110°C; 4 h;
参考文献
Bernini, Roberta; Cacchi, Sandro; Fabrizi, Giancarlo; Forte, Giovanni; Petrucci, Francesco; Prastaro, Alessandro; Niembro, Sandra; Shafir, Alexandr; Vallribera, Adelina
Green Chemistry, 2010 , vol. 12, # 1 p. 150 - 158
反应条件
potassium phosphate; 1,3-bis-(diphenylphosphino)propane; oxygen; palladium diacetate in methanol T=60°C; P=760.051 Torr; 4 h;
参考文献
Arcadi, Antonio; Cacchi, Sandro; Fabrizi, Giancarlo; Goggiamani, Antonella; Iazzetti, Antonia; Marinelli, Fabio
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 4 p. 545 - 548
反应条件
tetrakis(triphenylphosphine) palladium(0); tetra-(n-butyl)ammonium iodide; potassium carbonate in acetonitrile T=60°C; Inert atmosphereDarkness;
参考文献
Cacchi, Sandro; Fabrizi, Giancarlo; Goggiamani, Antonella; Perboni, Alcide; Sferrazza, Alessio; Stabile, Paolo
Organic Letters, 2010 , vol. 12, # 14 p. 3279 - 3281
反应条件
lithium hydroxide hydrate; C24H23N3O3PdS in N,N-dimethyl-formamide T=130°C; Larock Annulation; 24 h; Overall yield = 82 percent; regioselective reaction;
参考文献
Srinivas, Keesara; Saiprathima, Parvathaneni; Balaswamy, Kodicherla; Ra, Mandapati Mohan
Journal of Organometallic Chemistry, 2013 , vol. 741-742, # 1 p. 162 - 167
反应条件
potassium carbonate; [Pd(NH3)4](2+)/NaY zeolite in 1,4-dioxane Heating;
参考文献
Cusati, Giuseppe; Djakovitch, Laurent
Tetrahedron Letters, 2008 , vol. 49, # 16 p. 2499 - 2502
反应条件
18-crown-6 ether; potassium acetate in ethyl acetate T=20°C; 1 h;
参考文献
Benati, Luisa; Calestani, Gianluca; Leardini, Rino; Minozzi, Matteo; Nanni, Daniele; Spagnolo, Piero; Strazzari, Samantha; Zanardi, Giuseppe
Journal of Organic Chemistry, 2003 , vol. 68, # 9 p. 3454 - 3464
反应条件
1.1: i-Pr2NH; CuI / Pd(PPh3)2Cl2 / dimethylformamide 1.2: 87 percent / dimethylformamide / 1.5 h / 0 - 20 °C 2.1: tetrahydrofuran / 1.5 h / 0 °C 3.1: 80 percent / K2CO3 / Pd(PPh3)4 / acetonitrile / 3 h / 80 °C View Scheme
参考文献
Cacchi, Sandro; Fabrizi, Giancarlo; Parisi, Luca M.
Synthesis, 2004 , # 11 p. 1889 - 1894
反应条件
1: tetrahydrofuran / 1.5 h / 0 °C 2: 80 percent / K2CO3 / Pd(PPh3)4 / acetonitrile / 3 h / 80 °C View Scheme
参考文献
Cacchi, Sandro; Fabrizi, Giancarlo; Parisi, Luca M.
Synthesis, 2004 , # 11 p. 1889 - 1894
反应条件
1.1: i-Pr2NH; CuI / Pd(PPh3)2Cl2 / dimethylformamide 1.2: 87 percent / dimethylformamide / 1.5 h / 0 - 20 °C 2.1: tetrahydrofuran / 1.5 h / 0 °C 3.1: 80 percent / K2CO3 / Pd(PPh3)4 / acetonitrile / 3 h / 80 °C View Scheme
参考文献
Arcadi, Antonio; Cacchi, Sandro; Marinelli, Fabio
Tetrahedron Letters, 1992 , vol. 33, # 27 p. 3915 - 3918
反应条件
1: trifluoromethanesulfonyl azide; copper(II) sulfate; triethylamine / methanol; dichloromethane; water / 16 h / 20 °C / Inert atmosphere 2: dirhodium(II) tetrakis(perfluorobutyrate) / toluene / 16 h / 80 °C / Inert atmosphere; Molecular sieve View Scheme
参考文献
Sun, Ke; Liu, Sheng; Bec, Patryk M.; Driver, Tom G.
Angewandte Chemie - International Edition, 2011 , vol. 50, # 7 p. 1702 - 1706
