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乙二醇
甲醛
63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
143360-89-8
合成路线
（共 53 条）
143321-89-5
+
536-74-3
苯乙炔
→
反应条件
143360-89-8
反应条件
copper(l) iodide; N-methylpyrrolidine-2-carboxamide hydrochloride; caesium carbonate in N,N-dimethyl-formamide T=25°C; Sonogashira cross-coupling; 6 h; Inert atmosphere;
参考文献
Jiang, Huimin; Fu, Hua; Qiao, Renzhong; Jiang, Yuyang; Zhao, Yufen
Synthesis, 2008 , # 15 art. no. F06408SS, p. 2417 - 2426
13141-38-3
+
407-25-0
三氟乙酸酐
→
反应条件
143360-89-8
反应条件
pyridine in dichloromethane T=0 - 20°C;
参考文献
Swamy, Nalivela Kumara; Yazici, Arife; Pyne, Stephen G.
Journal of Organic Chemistry, 2010 , vol. 75, # 10 p. 3412 - 3419
143321-89-5
+
536-74-3
苯乙炔
→
反应条件
948-65-2
2-苯基吲哚
+
143360-89-8
反应条件
potassium phosphate; Cu[(phen)(PPh3)2]NO2 in 1,4-dioxane T=110°C; 24 h;
参考文献
Slough, Greg A.; Krchnak, Viktor; Helquist, Paul; Canham, Stephen M.
Organic Letters, 2004 , vol. 6, # 17 p. 2909 - 2912
615-43-0
2-碘苯胺
→
反应条件
143360-89-8
反应条件
1: CuI; triethylamine / Pd(Ph3P)2Cl2 / 20 °C 2: pyridine / CH2Cl2 / 0 - 20 °C View Scheme
参考文献
Cacchi, Sandro; Fabrizi, Giancarlo; Pace, Paola
Journal of Organic Chemistry, 1998 , vol. 63, # 4 p. 1001 - 1011
2727-71-1
+
536-74-3
苯乙炔
→
反应条件
143360-89-8
反应条件
DiPPF; palladium diacetate; potassium carbonate in N,N-dimethyl-formamide T=80°C; Sonogashira Cross-Coupling; 23 h; Inert atmosphereSealed tube;
参考文献
Lu, Bruce Z.; Wei, Han-Xun; Zhang, Yongda; Zhao, Wenyi; Dufour, Marine; Li, Guisheng; Farina, Vittorio; Senanayake, Chris H.
Journal of Organic Chemistry, 2013 , vol. 78, # 9 p. 4558 - 4562
536-74-3
苯乙炔
→
反应条件
143360-89-8
反应条件
1: CuI; triethylamine / Pd(Ph3P)2Cl2 / 20 °C 2: pyridine / CH2Cl2 / 0 - 20 °C View Scheme
参考文献
Cacchi, Sandro; Fabrizi, Giancarlo; Pace, Paola
Journal of Organic Chemistry, 1998 , vol. 63, # 4 p. 1001 - 1011
354-32-5
三氟乙酰氯
+
13141-38-3
→
反应条件
143360-89-8
反应条件
pyridine in dichloromethane T=0 - 20°C;
参考文献
Yin, Yan; Ma, Wenying; Chai, Zhuo; Zhao, Gang
Journal of Organic Chemistry, 2007 , vol. 72, # 15 p. 5731 - 5736
2727-71-1
+
536-74-3
苯乙炔
→
反应条件
948-65-2
2-苯基吲哚
+
143360-89-8
反应条件
bis(benzonitrile)palladium(II) dichloride; potassium acetate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in N,N-dimethyl-formamide T=80°C; Sonogashira Cross-Coupling; 1.2 h; Inert atmosphereSealed tube; regiospecific reaction;
参考文献
Lu, Bruce Z.; Wei, Han-Xun; Zhang, Yongda; Zhao, Wenyi; Dufour, Marine; Li, Guisheng; Farina, Vittorio; Senanayake, Chris H.
Journal of Organic Chemistry, 2013 , vol. 78, # 9 p. 4558 - 4562
108-86-1
溴代苯
+
2727-71-1
+
536-74-3
苯乙炔
→
反应条件
948-65-2
2-苯基吲哚
+
3469-20-3
2,3-二苯基吲哚
+
143360-89-8
反应条件
1: 2-bromo-N-(trifluoroacetyl)aniline; phenylacetylene With bis(benzonitrile)palladium(II) dichloride; caesium carbonate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in N,N-dimethyl-formamide T=80°C; Sonogashira Cross-Coupling; 5 h; Inert atmosphereSealed tube; 2: bromobenzene in N,N-dimethyl-formamide T=80°C; 8 h; Inert atmosphereSealed tube; regiospecific reaction;
参考文献
Lu, Bruce Z.; Wei, Han-Xun; Zhang, Yongda; Zhao, Wenyi; Dufour, Marine; Li, Guisheng; Farina, Vittorio; Senanayake, Chris H.
Journal of Organic Chemistry, 2013 , vol. 78, # 9 p. 4558 - 4562
108-86-1
溴代苯
+
2727-71-1
+
536-74-3
苯乙炔
→
反应条件
3469-20-3
2,3-二苯基吲哚
+
143360-89-8
反应条件
1: 2-bromo-N-(trifluoroacetyl)aniline; phenylacetylene With palladium diacetate; caesium carbonate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in N,N-dimethyl-formamide T=80°C; Sonogashira Cross-Coupling; 1.5 h; Inert atmosphereSealed tube; 2: bromobenzene in N,N-dimethyl-formamide T=80°C; 2 h; Inert atmosphereSealed tube; Reagent/catalystTime; regiospecific reaction;
参考文献
Lu, Bruce Z.; Wei, Han-Xun; Zhang, Yongda; Zhao, Wenyi; Dufour, Marine; Li, Guisheng; Farina, Vittorio; Senanayake, Chris H.
Journal of Organic Chemistry, 2013 , vol. 78, # 9 p. 4558 - 4562
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