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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
143360-89-8
合成路线
（共 53 条）
637-87-6
对氯碘苯
+
143360-89-8
→
反应条件
143360-82-1
3-(4-氯苯基)-2-苯基吲哚
反应条件
potassium carbonate in acetonitrile T=110°C; 4 h;
参考文献
Bernini, Roberta; Cacchi, Sandro; Fabrizi, Giancarlo; Forte, Giovanni; Petrucci, Francesco; Prastaro, Alessandro; Niembro, Sandra; Shafir, Alexandr; Vallribera, Adelina
Green Chemistry, 2010 , vol. 12, # 1 p. 150 - 158
1679-18-1
4-氯苯硼酸
+
143360-89-8
→
反应条件
143360-82-1
3-(4-氯苯基)-2-苯基吲哚
反应条件
potassium phosphate; 1,3-bis-(diphenylphosphino)propane; oxygen; palladium diacetate in methanol T=60°C; P=760.051 Torr; 4 h;
参考文献
Arcadi, Antonio; Cacchi, Sandro; Fabrizi, Giancarlo; Goggiamani, Antonella; Iazzetti, Antonia; Marinelli, Fabio
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 4 p. 545 - 548
673-41-6
+
143360-89-8
→
反应条件
143360-82-1
3-(4-氯苯基)-2-苯基吲哚
反应条件
tetrakis(triphenylphosphine) palladium(0); tetra-(n-butyl)ammonium iodide; potassium carbonate in acetonitrile T=60°C; Inert atmosphereDarkness;
参考文献
Cacchi, Sandro; Fabrizi, Giancarlo; Goggiamani, Antonella; Perboni, Alcide; Sferrazza, Alessio; Stabile, Paolo
Organic Letters, 2010 , vol. 12, # 14 p. 3279 - 3281
143360-89-8
→
反应条件
25365-71-3
2-苯基吲哚-3-甲醛
反应条件
1: 70 percent / Cs2CO3 / Pd(PPh3)4 / acetonitrile / 2 h / 100 °C 2: 100 percent / acetonitrile / 12 h / 90 °C 3: 78 percent / NaBH4 / methanol / -10 °C 4: 61 percent / CuO; aq. CuCl2 / acetonitrile View Scheme
参考文献
Cacchi, Sandro; Fabrizi, Giancarlo; Lamba, Doriano; Marinelli, Fabio; Parisi, Luca M.
Synthesis, 2003 , # 5 p. 728 - 734
143360-89-8
→
反应条件
2415-33-0
反应条件
(4-methoxyphenyl)-boronic acid; oxygen; palladium diacetate; potassium carbonate; triphenylphosphine in methanol T=80°C; P=760.051 Torr; 2 h;
参考文献
Arcadi, Antonio; Cacchi, Sandro; Fabrizi, Giancarlo; Goggiamani, Antonella; Iazzetti, Antonia; Marinelli, Fabio
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 4 p. 545 - 548
932-88-7
(碘乙炔基)苯
+
143360-89-8
→
反应条件
反应条件
potassium carbonate; tetrakis(triphenylphosphine) palladium(0) in acetonitrile T=80°C; 1 h;
参考文献
Arcadi, Antonio; Cacchi, Sandro; Fabrizi, Giancarlo; Marinelli, Fabio; Parisi, Luca M.
Journal of Organic Chemistry, 2005 , vol. 70, # 16 p. 6213 - 6217
5720-07-0
4-甲氧基苯硼酸
+
143360-89-8
→
反应条件
948-65-2
2-苯基吲哚
+
5834-42-4
+
2415-33-0
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; oxygen; palladium diacetate; potassium carbonate in methanol T=80°C; P=760.051 Torr; 6 h;
参考文献
Arcadi, Antonio; Cacchi, Sandro; Fabrizi, Giancarlo; Goggiamani, Antonella; Iazzetti, Antonia; Marinelli, Fabio
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 4 p. 545 - 548
33948-36-6
1-(4-喹啉基)甲胺
+
143360-89-8
→
反应条件
948-65-2
2-苯基吲哚
+
1224449-77-7
+
2415-33-0
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate in acetonitrile T=80°C; 2 h;
参考文献
Arcadi, Antonio; Cianci, Roberto; Ferrara, Giovanni; Marinelli, Fabio
Tetrahedron, 2010 , vol. 66, # 13 p. 2378 - 2383
33948-36-6
1-(4-喹啉基)甲胺
+
143360-89-8
→
反应条件
1224449-77-7
+
2415-33-0
反应条件
tris-(dibenzylideneacetone)dipalladium(0); triphenyl-arsane; caesium carbonate in acetonitrile T=100°C; 2 h;
参考文献
Arcadi, Antonio; Cianci, Roberto; Ferrara, Giovanni; Marinelli, Fabio
Tetrahedron, 2010 , vol. 66, # 13 p. 2378 - 2383
108-86-1
溴代苯
+
143360-89-8
→
反应条件
948-65-2
2-苯基吲哚
+
3469-20-3
2,3-二苯基吲哚
+
2415-33-0
反应条件
potassium carbonate; triphenylphosphine; tris(dibenzylideneacetone)dipalladium (0) in acetonitrile T=80°C; 8 h; Product distribution; Further Variations:ReagentsCatalystsTemperaturesSolvents;
参考文献
Cacchi, Sandro; Fabrizi, Giancarlo; Lamba, Doriano; Marinelli, Fabio; Parisi, Luca M.
Synthesis, 2003 , # 5 p. 728 - 734
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