tris-(dibenzylideneacetone)dipalladium(0); lithium tert-butylate; dicyclohexyl(2',6'-diisopropoxy-[1,1'-biphenyl]-2-yl)phosphine in 1,4-dioxane; water T=110°C; 12 h; Microwave irradiationInert atmosphere;

tris-(dibenzylideneacetone)dipalladium(0); lithium tert-butylate; dicyclohexyl(2',6'-diisopropoxy-[1,1'-biphenyl]-2-yl)phosphine in 1,4-dioxane; water T=110°C; 12 h; Microwave irradiationInert atmosphere; Reagent/catalystTemperature;

tris-(dibenzylideneacetone)dipalladium(0); lithium tert-butylate; dicyclohexyl(2',6'-diisopropoxy-[1,1'-biphenyl]-2-yl)phosphine in 1,4-dioxane; water T=110°C; 12 h; Microwave irradiationInert atmosphere;

tris-(dibenzylideneacetone)dipalladium(0); lithium chloride; lithium tert-butylate; dicyclohexyl(2',6'-diisopropoxy-[1,1'-biphenyl]-2-yl)phosphine in 1,4-dioxane; water T=110°C; 12 h; Microwave irradiationInert atmosphere;

1: tris-(dibenzylideneacetone)dipalladium(0); dicyclohexyl(2',6'-diisopropoxy-[1,1'-biphenyl]-2-yl)phosphine; lithium tert-butylate / water; 1,4-dioxane / 1 h / 110 °C / |Inert atmosphere; |Microwave irradiation 2: tris-(dibenzylideneacetone)dipalladium(0); dicyclohexyl(2',6'-diisopropoxy-[1,1'-biphenyl]-2-yl)phosphine; lithium tert-butylate / water; 1,4-dioxane / 12 h / 110 °C / |Inert atmosphere; |Microwave irradiation View Scheme

tris-(dibenzylideneacetone)dipalladium(0); lithium tert-butylate; dicyclohexyl(2',6'-diisopropoxy-[1,1'-biphenyl]-2-yl)phosphine in 1,4-dioxane; water T=110°C; 12 h; Microwave irradiationInert atmosphere;