(S)-1-氨基-3-(9h-咔唑-4-氧基)-2-丙醇合成路线 （共 6 条）
反应条件
ammonium formate; palladium in methanol
参考文献
Eli Lilly and Company
Patent: US6140352 A1, 2000 ;
US 6140352 A
反应条件
palladium 10 on activated carbon in methanol P=3102.97 - 3620.13 Torr; 6 h; Inert atmosphere;
参考文献
Krishna Reddy; Ramamohan; Ganesh; Srinivas; Mukkanti; Madhusudhan
Asian Journal of Chemistry, 2012 , vol. 24, # 8 p. 3468 - 3472
反应条件
ammonia in methanol T=25°C;
参考文献
Madhusudhan; Kumar, B. Anand; Chintamani; Rao, M. Narasimha; Udaykiran; Suresh; Kumar, V. Kiran; Mukkanti
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2010 , vol. 49, # 5 p. 606 - 610
反应条件
1: AlCl3, aluminium chloride / o-xylene / 120 °C / Inert atmosphere 2: palladium 10 on activated carbon / methanol / 6 h / 3102.97 - 3620.13 Torr / Inert atmosphere View Scheme
参考文献
Tatendra Reddy; Suneel Kumar; Omprakash; Dubey
Indian Journal of Heterocyclic Chemistry, 2012 , vol. 21, # 3 p. 251 - 254
反应条件
potassium carbonate in toluene T=80 - 85°C;
参考文献
Indian Journal of Heterocyclic Chemistry, , vol. 21, # 3 p. 251 - 254
反应条件
1: 0 °C / Reflux; basic condition; Inert atmosphere 2: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 25 h / 25 - 100 °C / Inert atmosphere 3: sodium hydroxide / ethanol / 12 h / Reflux; Inert atmosphere View Scheme
参考文献
Asian Journal of Chemistry, , vol. 24, # 8 p. 3468 - 3472
