(1,3,3-三甲基-2-亚甲基-2,3-二氢-1H-吲哚-6-基)-甲醇合成路线 （共 4 条）
反应条件
sodium hydroxide 1) ether, reflux, 12 h, 2) H2O; Yield given. Multistep reaction;
参考文献
WISCONSIN ALUMNI RESEARCH FOUNDATION
Patent: US2007/195309 A1, 2007 ;
Location in patent: Page/Page column 46; 47; 49 ;
反应条件
1.1: HCl; NaNO2; SnCl2*2H2O / H2O / 0.5 h / 0 °C 2.1: 131 mg / H2SO4 / 17 h / Heating 3.1: CH2Cl2 / 12 h / Heating 3.2: NaOH / H2O / 0.25 h View Scheme
参考文献
Inouye, Masahiko; Ueno, Masaru; Tsuchiya, Kikuo; Nakayama, Naomi; Konishi, Takashi; Kitao, Teijiro
Journal of Organic Chemistry, 1992 , vol. 57, # 20 p. 5377 - 5383
反应条件
1.1: 131 mg / H2SO4 / 17 h / Heating 2.1: CH2Cl2 / 12 h / Heating 2.2: NaOH / H2O / 0.25 h View Scheme
参考文献
Inouye, Masahiko; Ueno, Masaru; Tsuchiya, Kikuo; Nakayama, Naomi; Konishi, Takashi; Kitao, Teijiro
Journal of Organic Chemistry, 1992 , vol. 57, # 20 p. 5377 - 5383
反应条件
1: acetic acid / 2 h / 100 °C 2: 2) NaOH / 1) ether, reflux, 12 h, 2) H2O View Scheme
参考文献
Inouye, Masahiko; Ueno, Masaru; Tsuchiya, Kikuo; Nakayama, Naomi; Konishi, Takashi; Kitao, Teijiro
Journal of Organic Chemistry, 1992 , vol. 57, # 20 p. 5377 - 5383
