2-苄基-3-(二甲基氨基)丙烯醛合成路线 (共 3 条)
反应条件
1: With phosphorus pentachloride T=0 - 75°C; 1.75 h; 2: With N,N-dimethyl-formamide T=20°C; 72 h; 3: With sodium hydroxide in water T=0°C; pH=8;
参考文献
US2009/82352 A1, ;
Page/Page column 22 ;
US 20090082352 A1
反应条件
1: 2-benzyloxyacetaldehyde diethyl acetal With phosphorus pentachloride T=0 - 75°C; 2.08333 h; 2: N,N-dimethyl-formamide T=20°C; 72 h; 3: With sodium hydroxide in water pH=>= 8;
参考文献
US2009/62306 A1, ;
Page/Page column 26 ;
反应条件
sodium hydride in 1-methyl-pyrrolidin-2-one
T=0 - 80°C; 1 h;
参考文献
KOWA COMPANY, LTD.
Patent: US2009/82352 A1, 2009 ;
Location in patent: Page/Page column 22 ;
US 20090082352 A1