3-甲基-4-(苯基偶氮)苯酚合成路线 （共 6 条）
反应条件
1: aniline With hydrogenchloride; sodium nitrite in water T=0 - 5°C; 2: 3-methyl-phenol With sodium hydroxide in ethanol; water T=0 - 5°C;
参考文献
Xu, Hui; Zeng, Xiwen
Bioorganic and Medicinal Chemistry Letters, 2010 , vol. 20, # 14 p. 4193 - 4195
反应条件
antimony(V) pentachloride 1.) CCl4, overnight; 2.) nitromethane, 81-83 deg C, 3 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Yamamoto, Jiro; Nishigaki, Yukihiro; Umezu, Masahiro; Matsuura, Teruo
Tetrahedron, 1980 , vol. 36, p. 3177 - 3180
参考文献
Noelting; Kohn
Chemische Berichte, 1884 , vol. 17, p. 363
Full Text Show Details
Goldschmidt; Keppeler
Chemische Berichte, 1900 , vol. 33, p. 898
反应条件
in water 0.166667 h; pH 10.5;
参考文献
Bagal, I. L.; Zul'figarov, O. S.; Yurchenko, V. V.; Trachevskii, V. V.; El'tsov, A. V.
J. Gen. Chem. USSR (Engl. Transl.), 1992 , vol. 62, # 4.2. p. 928 - 934,762 - 767
参考文献
Noelting; Kohn
Chemische Berichte, 1884 , vol. 17, p. 363
参考文献
Noelting; Kohn
Chemische Berichte, 1884 , vol. 17, p. 363
