2,3,4,6-四-O-苄基-α-D-吡喃葡萄糖基 N,N,N',N'-四甲基二氨基磷酸酯合成路线 （共 2 条）
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; n-butyllithium in tetrahydrofuran T=-10°C; 2 h;
参考文献
Hashimoto, Shun-Ichi; Sakamoto, Hiroki; Honda, Takeshi; Ikegami, Shiro
Tetrahedron Letters, 1997 , vol. 38, # 29 p. 5181 - 5184
反应条件
n-butyllithium 1) THF, hexane, -78 deg C, 15 min, 2) HMPA, a) to -30 deg C, 0.5 h, b) -30 deg C, 2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Hashimoto; Yanagiya; Honda; Harada; Ikegami
Tetrahedron Letters, 1992 , vol. 33, # 24 p. 3523 - 3526
