[双(三氟乙酰基)碘]五氟苯合成路线 （共 10 条）
反应条件
nitric acid at -30°C, then warming to 20°C, stirring;
参考文献
Schmeisser, M.; Dahmen, K.; Sartori, P.
Chemische Berichte, 1967 , vol. 100, p. 1633 - 1637
反应条件
Oxonereg; in chloroform T=20°C; 2 h;
参考文献
Zagulyaeva, Aleksandra A.; Yusubov, Mekhman S.; Zhdankin, Viktor V.
Journal of Organic Chemistry, 2010 , vol. 75, # 6 p. 2119 - 2122
反应条件
in dichloromethane T=-40 - 20°C; 8 h;
参考文献
Page, T. Keri; Wirth, Thomas
Synthesis, 2006 , # 18 p. 3153 - 3155
参考文献
F: PerFHalOrg.SVol.3, 7, page 253 - 267
反应条件
sodium hydrogencarbonate 20 h;
参考文献
Spyroudis, Spyros; Varvoglis, Anastasios
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 2 p. 135 - 137
反应条件
dimethylsulfoxide-d6 T=20°C; 1.58333 h; Inert atmosphere;
参考文献
Schaefer, Sascha; Wirth, Thomas
Angewandte Chemie - International Edition, 2010 , vol. 49, # 15 p. 2786 - 2789
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.3, 7, page 253 - 267
反应条件
water in further solvent(s) with satd. NaHCO3;
参考文献
Chemische Berichte, , vol. 100, p. 1633 - 1637
反应条件
dimethylsulfoxide-d6 T=20°C; 1.58333 h; Inert atmosphere;
参考文献
Schaefer, Sascha; Wirth, Thomas
Angewandte Chemie - International Edition, 2010 , vol. 49, # 15 p. 2786 - 2789
反应条件
1: 10 percent / acetonitrile / Ambient temperature; 1 week
2: NaN3 / acetonitrile / 5 h / 60 °C
View Scheme
参考文献
Spyroudis, Spyros; Varvoglis, Anastasios
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 2 p. 135 - 137
