N-[1-(氨基甲基)环己基]苯胺合成路线 (共 3 条)
参考文献
Omran; Moustafa
Phosphorus, Sulfur and Silicon and the Related Elements, 2006 , vol. 181, # 11 p. 2519 - 2528
反应条件
borane-dimethylsulphate in tetrahydrofuran T=20°C; 17 h; Heating / reflux; Product distribution / selectivity;
参考文献
GALDERMA RESEARCH and DEVELOPMENT
Patent: WO2009/30750 A1, 2009 ;
Location in patent: Page/Page column 30-31 ;
WO 2009/030750 A1
反应条件
1: 80 percent / glacial acetic acid / H2O / 0.5 h / 0 °C 2: H2, methanolic NH3 / Raney nickel / 1875.1 Torr / Ambient temperature View Scheme
参考文献
Naim, S. Shawkat; Sharma, Satyavan
Synthesis, 1992 , # 7 p. 664 - 666