1-(2-环戊烯-1-基)-2,4(1H,3H)-嘧啶二酮合成路线 （共 3 条）
反应条件
trimethylsilyl trifluoromethanesulfonate; [bis(acetoxy)iodo]benzene in dichloromethane T=20°C; 1 h;
参考文献
Yoshimura, Yuichi; Ohta, Masatoshi; Imahori, Tatsushi; Imamichi, Tomozumi; Takahata, Hiroki
Organic Letters, 2008 , vol. 10, # 16 p. 3449 - 3452
反应条件
trimethylsilyl trifluoromethanesulfonate; [bis(acetoxy)iodo]benzene in dichloromethane T=20°C; 15 h;
参考文献
Yoshimura, Yuichi; Ohta, Masatoshi; Imahori, Tatsushi; Imamichi, Tomozumi; Takahata, Hiroki
Organic Letters, 2008 , vol. 10, # 16 p. 3449 - 3452
反应条件
sodium hydride; 1,2-bis-(diphenylphosphino)ethane; bis(dibenzylideneacetone)-palladium(0) 1.) THF, 45 deg C, 5 min, 2.) THF, DMF, 60 deg C, 24 h; Yield given. Multistep reaction;
参考文献
Liotta, Fina; Unelius, C. Rikard; Kozak, Janusz; Norin, Torbjoern
Acta Chemica Scandinavica, 1992 , vol. 46, # 7 p. 686 - 688
