反应条件
1.1: NaH / dimethylformamide / 1 h / 20 °C
1.2: 85 percent / dimethylformamide / 24 h / 25 °C
2.1: 73 percent / ICl; NaN3 / acetonitrile; dimethylformamide / 70 h / Heating
3.1: 64 percent / toluene / 1 h
4.1: 94 percent / 2,6-lutidine; TMSOTf / CH2Cl2 / 0.75 h / 20 °C
5.1: 83 percent / pyridine / 0.5 h / 20 °C
6.1: 83 percent / LiAlH4 / diethyl ether / 2 h / Heating
View Scheme
参考文献
Pedersen, Hanne; Sinning, Steffen; Buelow, Anne; Wiborg, Ove; Falborg, Lise; Bols, Mikael
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 19 p. 2861 - 2869
