反应条件
1: SO2Cl2 / CH2Cl2 / 0.5 h / 20 °C
2: 20.1 g / aq. HCOOH / 0.33 h / 80 °C
3: 77.2 percent / NaBH4 / CH2Cl2; methanol / 0.5 h / 0 °C
4: H2 / Pd/C / methanol / 4.5 h / 5 °C
5: aq. Na2CO3 / CH2Cl2 / 1 h / 20 °C
6: K2CO3 / methanol / 6 h / 20 °C
7: 7.55 g / ethanol / 3 h / Heating
8: aq. K2CO3 / CH2Cl2 / 8 h / 20 °C
View Scheme
参考文献
Honda, Yutaka; Katayama, Satoshi; Kojima, Mitsuhiko; Suzuki, Takayuki; Kishibata, Naomi; Izawa, Kunisuke
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 14 p. 2061 - 2070
