2,2-亚甲基 双(4,6-二叔丁基苯酚)合成路线 （共 13 条）
反应条件
potassium hydroxide in tert-butyl alcohol T=100°C; 5 h;
参考文献
Belostoskaya, I. S.; Komissarova, N. L.; Shubina, O. V.; Grishina, E. A.; Ershov, V. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 9.2. p. 1980 - 1981
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , vol. 39, # 9 p. 2171
反应条件
1: 2,4-di-tert-butylphenol; methylmagnesium bromide in diethyl ether T=0°C; 2: formaldehyd in toluene 12 h; Heating; Further stages.;
参考文献
Davis; Balsells; Carroll; Walsh
Organic letters, 2001 , vol. 3, # 14 p. 2161 - 2164
反应条件
montmorillonite KSF in n-heptane 2 h; Reflux;
参考文献
Buravlev, Evgeny V.; Chukicheva, Irina Yu.; Borisenkov, Mikhail F.; Kutchin, Aleksandr V.
Synthetic Communications, 2012 , vol. 42, # 24 p. 3670 - 3676,7
Title/Abstract Full Text Show Details
Buravlev, Evgeny V.; Chukicheva, Irina Yu.; Borisenkov, Mikhail F.; Kutchin, Aleksandr V.
Synthetic Communications, 2012 , vol. 42, # 24 p. 3670 - 3676
反应条件
montmorillonite KSF in toluene Reflux;
参考文献
Buravlev, Evgeny V.; Chukicheva, Irina Yu.; Borisenkov, Mikhail F.; Kutchin, Aleksandr V.
Synthetic Communications, 2012 , vol. 42, # 24 p. 3670 - 3676,7
Title/Abstract Full Text Show Details
Buravlev, Evgeny V.; Chukicheva, Irina Yu.; Borisenkov, Mikhail F.; Kutchin, Aleksandr V.
Synthetic Communications, 2012 , vol. 42, # 24 p. 3670 - 3676
参考文献
Gurvich; Yakov Abramovich; Grinberg; Alexandr Afroimovich; Liakumovich; Alexandr Grigorievich; Michurov; Jury Ivanovich; Starikova; Olga Fedorovna; Yanshevsky; Vladimir Avgustovich; Kumok; Simona Tevievna; Styskin; Evgeny Lvovich; Rutman; Grigory Iosifich
Patent: US4087469 A1, 1978 ;
反应条件
toluene-4-sulfonic acid Heating;
参考文献
Ohba, Yoshihiro; Ito, Kazuaki; Maeda, Hiroyuki; Ebara, Hiroaki; Takaki, Shin; Nagasawa, Tomomi
Bulletin of the Chemical Society of Japan, 1998 , vol. 71, # 10 p. 2393 - 2402
反应条件
1: 58 percent / aq. NaOH / methanol / 5 h / 45 °C 2: 59 percent / p-toluenesulfonic acid / Heating View Scheme
参考文献
Ohba, Yoshihiro; Ito, Kazuaki; Maeda, Hiroyuki; Ebara, Hiroaki; Takaki, Shin; Nagasawa, Tomomi
Bulletin of the Chemical Society of Japan, 1998 , vol. 71, # 10 p. 2393 - 2402
反应条件
acetic acid; 4-hydroxymethyl-N,N-dimethylaniline 48 h; Heating;
参考文献
Kochansky, Jan; Cohen, Charles F.; Lusby, William R.
Journal of Agricultural and Food Chemistry, 1995 , vol. 43, # 11 p. 2974 - 2980
反应条件
formic acid; acetic acid 48 h; Heating;
参考文献
Kochansky, Jan; Cohen, Charles F.; Lusby, William R.
Journal of Agricultural and Food Chemistry, 1995 , vol. 43, # 11 p. 2974 - 2980
反应条件
1: concentrated sulfuric acid; benzene / 50 °C / Einleiten von 2-Methyl-propen 2: sulfuric acid / 95 - 100 °C View Scheme
参考文献
Wegler; Faber
Chemische Berichte, 1949 , vol. 82, p. 327,332
