in methanol slow addn. of copper compd. to methanol soln. of nitrogen compd., stirring for 1 h at room temp.; filtration, washing with methanol, crystn. from CH2Cl2/acetone (1:1), elem. anal.;
参考文献
Vahdat, Seyed Mohammad
Combinatorial Chemistry and High Throughput Screening, 2013 , vol. 16, # 10 p. 782 - 787
in ethanol to soln. of ligand in EtOH was added soln. of metal acetate in EtOH; mixt. refluxed for 2 h; cooled; ppt. filtered off; recrystd. (CHCl3/EtOH, 1:2); dried (vac.); elem. anal.;
methanol; aniline in chloroform Kinetics; room temperature; not isolated; ESR-spectroscopy;
参考文献
Talzi, E. P.; Nekipelov, V. M.; Zamaraev, K. I.
Russian Journal of Physical Chemistry (Translation of Zhurnal Fizicheskoi Khimii), 1984 , vol. 58, p. 165 - 178
Zhurnal Fizicheskoi Khimii, 1984 , vol. 58, p. 273 - 291
in neat (no solvent) simultanous thermal vaporisation (1E-4 mmHg); vibrational spectroscopy;
参考文献
Kuzharov, A. S.; Kut'kov, A. A.; Suchkov, V. V.
Russian Journal of Physical Chemistry, 1980 , vol. 54, # 12 p. 1784 - 1786
Zhurnal Fizicheskoi Khimii, 1980 , vol. 54, p. 3118 - 3122
KOH in ethanol soln. of Cu(ClO4)2 and N-salicylideneaniline heated under reflux 0.5 h, when added soln. of di-2-pyridylamine, heated 1 h, the mixt. cooled; ppt. washed (benzene); IR;
参考文献
Garland, M. T.; Le Marouille, J. Y.; Spodine, E.
Acta Crystallographica, Section C: Crystal Structure Communications, 1986 , vol. 42, p. 299 - 301
in methanol Kinetics; byproducts: C6H4OH(CHNC(CH3)3); at 25°C, for 72 h;
参考文献
Elias, Horst; Muth, Horst; Niederhoefer, Beate; Wannowius, Klaus J.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1981 , p. 1825 - 1830
in ethanol; water Schiff base soln. in ethanol added to hot soln. of copper(II) acetate in hot aq. ethanol in molar ratio of 2:1; ppt. recrystd. from trichloromethane or ethanol; elem. anal.;
参考文献
Harries, H. J.; Orford, B. F.; Burgess, J.
Inorganica Chimica Acta, 1983 , vol. 68, p. 41 - 44
