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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
143702-29-8
合成路线
（共 8 条）
143702-29-8
→
反应条件
3189-13-7
6-甲氧基吲哚
反应条件
1: 94 percent / xylene / Heating 2: 99 percent / aq. NaOH / Heating 3: 87 percent / Cu; quinoline / Heating View Scheme
参考文献
Allen; Hamaker; La Loggia; Cook
Synthetic Communications, 1992 , vol. 22, # 14 p. 2077 - 2102
143702-29-8
→
反应条件
143702-30-1
反应条件
1: 89 percent / xylene / 9 h / Heating 2: 93.9 percent / 2N aq. NaOH / 0.5 h / Heating 3: 97.6 percent / Cu / quinoline / 2 h / Heating 4: 1.) POCl3, 3.) aq. NaOH 5: 1.) NaH / 1.) THF, 40 deg C, 90 min, 2.) THF, RT, 18 h View Scheme
参考文献
Allen; Hamaker; La Loggia; Cook
Synthetic Communications, 1992 , vol. 22, # 14 p. 2077 - 2102
143702-29-8
→
反应条件
98081-83-5
6-甲氧基-1H-吲哚-2-羧酸甲酯
反应条件
Rh2(O2CC3F7)4 in toluene T=40°C; 16 h;
参考文献
Stokes, Benjamin J.; Dong, Huijun; Leslie, Brooke E.; Pumphrey, Ashley L.; Driver, Tom G.
Journal of the American Chemical Society, 2007 , vol. 129, # 24 p. 7500 - 7501
143702-29-8
→
反应条件
70555-46-3
6-甲氧基吲哚-3-甲醛
反应条件
1: 94 percent / xylene / Heating 2: 99 percent / aq. NaOH / Heating 3: 87 percent / Cu; quinoline / Heating 4: 89 percent / phosphoryl chloride / 0 - 40 °C View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 47, # 25 p. 6270 - 6282
143702-29-8
→
反应条件
16732-73-3
6-甲氧基吲哚-2-羧酸
反应条件
1: 94 percent / xylene / Heating 2: 99 percent / aq. NaOH / Heating View Scheme
参考文献
Allen; Hamaker; La Loggia; Cook
Synthetic Communications, 1992 , vol. 22, # 14 p. 2077 - 2102
143702-29-8
→
反应条件
651331-51-0
反应条件
1.1: 94 percent / xylene / Heating 2.1: 99 percent / aq. NaOH / Heating 3.1: 87 percent / Cu; quinoline / Heating 4.1: 89 percent / phosphoryl chloride / 0 - 40 °C 5.1: NaOH / CH2Cl2 / 20 °C 5.2: 97 percent / CH2Cl2 / 20 °C View Scheme
参考文献
Coowar, Djalil; Bouissac, Julien; Hanbali, Mazen; Paschaki, Marie; Mohier, Eliane; Luu, Bang
Journal of Medicinal Chemistry, 2004 , vol. 47, # 25 p. 6270 - 6282
143702-29-8
→
反应条件
651331-67-8
反应条件
1.1: 94 percent / xylene / Heating 2.1: 99 percent / aq. NaOH / Heating 3.1: 87 percent / Cu; quinoline / Heating 4.1: 89 percent / phosphoryl chloride / 0 - 40 °C 5.1: NaOH / CH2Cl2 / 20 °C 5.2: 97 percent / CH2Cl2 / 20 °C 6.1: n-BuLi / tetrahydrofuran; hexane / 0 °C 6.2: potassium tert-butoxide / tetrahydrofuran; hexane / 0 °C 6.3: 91 percent / tetrahydrofuran; hexane / -78 - 0 °C 7.1: 80 percent / H2 / Pd/C / ethanol / 20 °C / 760 Torr View Scheme
参考文献
Coowar, Djalil; Bouissac, Julien; Hanbali, Mazen; Paschaki, Marie; Mohier, Eliane; Luu, Bang
Journal of Medicinal Chemistry, 2004 , vol. 47, # 25 p. 6270 - 6282
143702-29-8
→
反应条件
651331-76-9
反应条件
1.1: 94 percent / xylene / Heating 2.1: 99 percent / aq. NaOH / Heating 3.1: 87 percent / Cu; quinoline / Heating 4.1: 89 percent / phosphoryl chloride / 0 - 40 °C 5.1: NaOH / CH2Cl2 / 20 °C 5.2: 97 percent / CH2Cl2 / 20 °C 6.1: n-BuLi / tetrahydrofuran; hexane / 0 °C 6.2: potassium tert-butoxide / tetrahydrofuran; hexane / 0 °C 6.3: 78 percent / tetrahydrofuran; hexane / -78 - 0 °C 7.1: 85 percent / H2 / Pd/C / ethanol / 20 °C / 760 Torr View Scheme
参考文献
Coowar, Djalil; Bouissac, Julien; Hanbali, Mazen; Paschaki, Marie; Mohier, Eliane; Luu, Bang
Journal of Medicinal Chemistry, 2004 , vol. 47, # 25 p. 6270 - 6282
