1: With tris((S,S)-3,4-diphenylpyrrolidino)sulfonium salt in diethyl ether
T=-78°C; trifluoromethylation; 24 h;
2: With hydrogenchloride in tetrahydrofuran
T=20°C; Hydrolysis; 1 h;
zinc in pyridine
T=20°C; P=1500.1 - 3000.2 Torr; 4 h;
参考文献
Tordeux, Marc; Francese, Catherine; Wakselman, Claude
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 7 p. 1951 - 1957