5-O-(3-甲基-2-丁烯基)山柰酚三-O-甲氧基甲基醚合成路线 (共 4 条)
反应条件
tetra(n-butyl)ammonium hydroxide in dichloromethane; toluene T=20°C;
参考文献
Daskiewicz, Jean-Baptiste; Depeint, Flore; Viornery, Lionel; Bayet, Christine; Comte-Sarrazin, Geraldine; Comte, Gilles; Gee, Jennifer M.; Johnson, Ian T.; Ndjoko, Karine; Hostettmann, Kurt; Barron, Denis
Journal of Medicinal Chemistry, 2005 , vol. 48, # 8 p. 2790 - 2804
反应条件
1: 52 percent / N,N-diisopropylethylamine / dimethylformamide / 20 °C 2: 75 percent / tetrabutylammonium hydroxide hydrate / CH2Cl2; toluene / 20 °C View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 48, # 8 p. 2790 - 2804
反应条件
potassium carbonate in methanol 10 h; Ambient temperature;
参考文献
Heterocycles, , vol. 34, # 6 p. 1213 - 1225
反应条件
1: 70 percent / N,N-diethylaniline / 217 °C 2: 73 percent / aq. HCl / methanol / Heating View Scheme
参考文献
Daskiewicz, Jean-Baptiste; Depeint, Flore; Viornery, Lionel; Bayet, Christine; Comte-Sarrazin, Geraldine; Comte, Gilles; Gee, Jennifer M.; Johnson, Ian T.; Ndjoko, Karine; Hostettmann, Kurt; Barron, Denis
Journal of Medicinal Chemistry, 2005 , vol. 48, # 8 p. 2790 - 2804