3-溴甲基苯基硼酸, 新戊二醇酯合成路线 （共 6 条）
反应条件
1: in cyclohexane 1.5 h; Heating / reflux; 2: With N-bromosuccinmide; dibenzoyl peroxide in cyclohexane 2 h; Heating / reflux;
参考文献
US2007/117983 A1, ;
Page/Page column 13 ;
反应条件
N-bromosuccinmide in tetrachloromethane 12 h; Reflux;
参考文献
Gorityala, Bala Kishan; Lu, Zhiqiang; Leow, Min Li; Ma, Jimei; Liu, Xue-Wei
Journal of the American Chemical Society, 2012 , vol. 134, # 37 p. 15229 - 15232
反应条件
1,3-dibromo-5,5-dimethyl-hydantoin; 2,2'-azo-bisisobutyronitrile in cyclohexane T=79°C;
参考文献
The Journal of organic chemistry, , vol. 68, # 13 p. 5168 - 5173
反应条件
1.1: n-BuLi / heptane; tetrahydrofuran / 0.75 h / -78 °C 1.2: B(Oi-Pr)3 / tetrahydrofuran; heptane / 2 h / -78 - -10 °C 1.3: 50 percent / acetic acid / tetrahydrofuran; heptane / -10 - 20 °C 2.1: 1,3-dibromo-5,5-dimethyl-imidazolidine-2,4-dione; AIBN / cyclohexane / 79 °C View Scheme
参考文献
The Journal of organic chemistry, , vol. 68, # 13 p. 5168 - 5173
反应条件
1.1: n-BuLi / heptane; tetrahydrofuran / 0.75 h / -78 °C 1.2: B(Oi-Pr)3 / tetrahydrofuran; heptane / 2 h / -78 - -10 °C 1.3: 50 percent / acetic acid / tetrahydrofuran; heptane / -10 - 20 °C 2.1: 1,3-dibromo-5,5-dimethyl-imidazolidine-2,4-dione; AIBN / cyclohexane / 79 °C View Scheme
参考文献
The Journal of organic chemistry, , vol. 68, # 13 p. 5168 - 5173
反应条件
1: toluene / 12 h / |Reflux 2: N-bromosuccinmide / tetrachloromethane / 12 h / |Reflux View Scheme
参考文献
Journal of the American Chemical Society, , vol. 134, # 37 p. 15229 - 15232
