2,3-二氢-1H-茚-1-羧酸合成路线 （共 37 条）
反应条件
hydrogen; palladium on activated charcoal in methanol T=20°C; P=2844.39 Torr; 18 h;
参考文献
Bristol-Myers Squibb Company
Patent: US2007/185056 A1, 2007 ;
Location in patent: Page/Page column 51 ;
US 20070185056 A1
反应条件
palladium on activated charcoal; hydrogen in methanol
参考文献
Pietruszka, Joerg; Simon, Robert Christian; Kruska, Fabian; Braun, Manfred
European Journal of Organic Chemistry, 2009 , # 35 p. 6217 - 6224
反应条件
trans-bis((o-trifluoromethylphenyl)tert-butylmethylphosphine)palladiumdichloride; water; toluene-4-sulfonic acid; lithium chloride in butanone T=80°C; P=22502.3 Torr; 24 h; Inert atmosphereAutoclave; regioselective reaction;
参考文献
Grabulosa, Arnald; Frew, Jamie J.R.; Fuentes, Jose A.; Slawin, Alexandra M.Z.; Clarke, Matthew L.
Journal of Molecular Catalysis A: Chemical, 2010 , vol. 330, # 1-2 p. 18 - 25
反应条件
hydrogen; palladium on activated charcoal in acetic acid 12 h;
参考文献
Kawasaki, Takayasu; Horimai, Emiko; Ohta, Hiromichi
Bulletin of the Chemical Society of Japan, 1996 , vol. 69, # 12 p. 3591 - 3594
反应条件
Ni(PCy3)2Cl2; tetra-(n-butyl)ammonium iodide; zinc in N,N-dimethyl acetamide T=20°C; P=760.051 Torr; Schlenk technique;
参考文献
Leon, Thierry; Correa, Arkaitz; Martin, Ruben
Journal of the American Chemical Society, 2013 , vol. 135, # 4 p. 1221 - 1224
反应条件
barium dihydroxide; ethanol; silver nitrate
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 170, p. 467
Bulletin de la Societe Chimique de France, , vol. <4> 27, p. 789
反应条件
hydrogen; palladium on activated charcoal 2.) THF, acetic acid, 25 deg C; Yield given. Multistep reaction;
参考文献
Journal of the American Chemical Society, , vol. 106, p. 3964
反应条件
sodium hydroxide 2 h; Heating;
参考文献
Nongrum, F.M.; Myrboh, B.
Synthesis, 1987 , # 9 p. 845 - 846
参考文献
Adir et Compagnie
Patent: US5194437 A1, 1993 ;
反应条件
1: 1.) BuLi / 1.) hexane, ether, room temperature, 10 min, 2.) -78 deg C, 15 min 2: 82 percent / H2 / Pd-C / acetic acid / 12 h View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 69, # 12 p. 3591 - 3594
