反应条件
1: 2,5-diiodothiophene-1,1-dioxide With tris-(dibenzylideneacetone)dipalladium(0); triphenyl-arsane in 1,4-dioxane
Stille Cross Coupling; 0.166667 h; Inert atmosphereSealed tube;
2: 2-trimethylstannylbenzene in 1,4-dioxane
T=100°C; Stille Cross Coupling; 6 h; Inert atmosphereSealed tube;
3: With tris-(dibenzylideneacetone)dipalladium(0); triphenyl-arsane in 1,4-dioxane
T=100°C; Stille Cross Coupling; Inert atmosphereSealed tube;
参考文献
Tsai, Chia-Hua; Chirdon, Danielle N.; Maurer, Andrew B.; Bernhard, Stefan; Noonan, Kevin J. T.
Organic Letters, 2013 , vol. 15, # 20 p. 5230 - 5233