4-(2-乙酰氨基基乙基)苯基乙酸酯合成路线 (共 6 条)
反应条件
triethylamine in dichloromethane T=0 - 20°C; 2 h;
参考文献
Yuhan Corporation
Patent: US6352993 B1, 2002 ;
Location in patent: Page column 11 ;
参考文献
E. Elgorashi, Esameldin; E. Drewes, Siegfried; Van Staden, Johannes
Phytochemistry, 2001 , vol. 56, # 6 p. 637 - 640
反应条件
1: 2-(4-hydroxyphenyl)ethylamine With sodium hydride in dichloromethane 0.25 h; Inert atmosphere; 2: acetyl chloride in dichloromethane T=20°C; 2 h; Inert atmosphere;
参考文献
Wild, Gareth. P.; Wiles, Charlotte; Watts, Paul; Haswell, Stephen J.
Tetrahedron, 2009 , vol. 65, # 8 p. 1618 - 1629
反应条件
sodium hydroxide in chloroform; water 1 h; Ambient temperature;
参考文献
Sakakibara, Tohru; Watabe, Yukie; Yamada, Masahide; Sudoh, Rokuro
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, # 1 p. 247 - 254
参考文献
Comin; Keller-Schierlein
Helvetica Chimica Acta, 1959 , vol. 42, p. 1730
反应条件
sodium hydroxide in methanol; water T=0°C; 0.166667 h;
参考文献
Yuhan Corporation
Patent: US6352993 B1, 2002 ;
Location in patent: Page column 11 ;