4,4’-氧代双苯甲酸二甲酯合成路线 （共 11 条）
反应条件
triethylamine; 1,4-di(diphenylphosphino)-butane; palladium dichloride in toluene T=120°C; P=7500.75 Torr; 10 h;
参考文献
Adchemco Corporation
Patent: EP1211235 A2, 2002 ;
Location in patent: Example 2 ;
反应条件
9,10-DIHYDRO-9,10-DIOXO-2,3-ANTHRACENEDICARBOXYLIC ACID; oxygen 48 h; Irradiation;
参考文献
Tada, Norihiro; Ikebata, Yuki; Nobuta, Tomoya; Hirashima, Shin-Ichi; Miura, Tsuyoshi; Itoh, Akichika
Photochemical and Photobiological Sciences, 2012 , vol. 11, # 4 p. 616 - 619
反应条件
potassium carbonate T=200 - 214°C;
参考文献
Angewandte Chemie, , vol. 82, p. 79 - 80
反应条件
T=200 - 270°C; Further byproducts given;
参考文献
Jost, Philippe; Forestiere, Alain; Sillion, Bernard; Le Perchec, Pierre
Tetrahedron Letters, 1982 , vol. 23, # 42 p. 4311 - 4314
反应条件
tetrafluoroboric acid; sodium nitrite; palladium diacetate 1.) 0 deg C, 2.) 25 deg C, 30 min; Yield given. Multistep reaction;
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 3 p. 407 - 410
反应条件
1: SOCl2 / 0.25 h / Heating 2: 1 h / Heating View Scheme
参考文献
Archiv der Pharmazie, , vol. 333, # 6 p. 181 - 188
反应条件
Esterification; 1 h; Heating;
参考文献
Archiv der Pharmazie, , vol. 333, # 6 p. 181 - 188
参考文献
Yakugaku Zasshi, , vol. 57, p. 609,614; dtsch. Ref. S. 131, 135
Chem.Abstr., , p. 2898
反应条件
1: 91 percent / LiAlH4 / tetrahydrofuran / 72 h / 0 °C 2: 69 percent / PPh3; NBS / tetrahydrofuran / 96 h / 20 °C View Scheme
参考文献
Shimizu, Linda S.; Hughes, Andrew D.; Smith, Mark D.; Davis, Matthew J.; Zhang, B. Paul; Zur Loye, Hans-Conrad; Shimizu, Ken D.
Journal of the American Chemical Society, 2003 , vol. 125, # 49 p. 14972 - 14973
反应条件
1: With lithium diisopropyl amide in tetrahydrofuran T=-78°C; 2: With acetic acid in tetrahydrofuran T=-78°C;
参考文献
BRISTOL-MYERS SQUIBB COMPANY; BELEMA, Makonen; HEWAWASAM, Piyasena
Patent: WO2012/39717 A1, 2012 ;
Location in patent: Page/Page column 51-52 ;
