2,3-二甲基-3-丁烯酸乙酯合成路线 (共 17 条)
参考文献
Huston; Goerner
Journal of the American Chemical Society, 1946 , vol. 68, p. 2505
反应条件
bromine; sodium ethanolate; tert-butyl alcohol Reagens 4: Aethanol;
参考文献
Adams; Gianturco
Journal of the American Chemical Society, 1957 , vol. 79, p. 166,169
反应条件
lithium diisopropyl amide in tetrahydrofuran
1.) -78 deg C, 1 h, 2.) -78 deg C -> room temperature, 1 h;
参考文献
Smith,A.B.; Toder,B.H.; Branca,S.J.
Journal of the American Chemical Society, 1981 , vol. 103, p. 1996
反应条件
1,2-dimethyl-1H-imidazole in diethyl ether
384 h; Irradiation;
参考文献
Duhaime, Randy M.; Lombardo, Domenic A.; Skinner, Ian A.; Weedon, Alan C.
Journal of Organic Chemistry, 1985 , vol. 50, # 6 p. 873 - 879
反应条件
1: BuLi, Zn / benzene; hexane / 2 h / Heating
2: phosphorus pentoxide / benzene / 4 h / Heating
View Scheme
参考文献
McCullough, John J.; MacInnis, W. Keith; Lock, Colin J. L.; Faggiani, Rommulo
Journal of the American Chemical Society, 1982 , vol. 104, # 17 p. 4644 - 4658
反应条件
P2O5 in benzene
4 h; Heating; Yield given;
参考文献
McCullough, John J.; MacInnis, W. Keith; Lock, Colin J. L.; Faggiani, Rommulo
Journal of the American Chemical Society, 1982 , vol. 104, # 17 p. 4644 - 4658
反应条件
phosphorus pentoxide; benzene
参考文献
Huston; Goerner
Journal of the American Chemical Society, 1946 , vol. 68, p. 2505
反应条件
1: sodium hydride; dioxane
2: potassium hydroxide; aqueous ethanol
3: pyridine
View Scheme
参考文献
Corey
Journal of the American Chemical Society, 1952 , vol. 74, p. 5897,5903
反应条件
1: potassium hydroxide; aqueous ethanol
2: pyridine
View Scheme
参考文献
Corey
Journal of the American Chemical Society, 1952 , vol. 74, p. 5897,5903
参考文献
Corey
Journal of the American Chemical Society, 1952 , vol. 74, p. 5897,5903