反式-1,2-二苯乙烯氧化物合成路线 (共 213 条)
反应条件
Bacillus megaterium ECU1001 cell-free extract in potassium phosphate buffer; dimethyl sulfoxide T=30°C; pH=7; 0.166667 h; Resolution of racemateEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Zhao, Jing; Chu, Yan-Yan; Li, Ai-Tao; Ju, Xin; Kong, Xu-Dong; Pan, Jiang; Tang, Yun; Xu, Jian-He
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 9 p. 1510 - 1518
反应条件
PTAB; antimony(III)tribromide in dimethyl sulfoxide T=20°C; 40 h; Product distribution; Further Variations:ReagentsSolventsreaction times, reagent ratios;
参考文献
Sayama, Shinsei
Tetrahedron Letters, 2006 , vol. 47, # 24 p. 4001 - 4005
反应条件
bis-[(trifluoroacetoxy)iodo]benzene in dichloromethane 24 h; Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 46, p. 5231 - 5233
反应条件
4 A molecular sieve; dimethyl sulfoxide; trifluoroacetic acid T=100°C; 9 h; in a sealed tube;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 62, # 2 p. 645 - 647
反应条件
trifluorormethanesulfonic acid; N-ethyl-N,N-diisopropylamine 1.) DMSO, 23 deg C; 2.) CH2Cl2, -78 deg C, then room temp.; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Trost, Barry M.; Fray, Jonathan M.
Tetrahedron Letters, 1988 , vol. 29, # 18 p. 2163 - 2166
反应条件
PTAB; N-benzyl-N,N,N-triethylammonium chloride; antimony(III)tribromide in dimethyl sulfoxide T=20°C; 46 h;
参考文献
Sayama, Shinsei
Tetrahedron Letters, 2006 , vol. 47, # 24 p. 4001 - 4005
反应条件
1,4-dioxane; ammonia; water T=120°C;
参考文献
Jankowski,K.; Berse,C.
Canadian Journal of Chemistry, 1967 , vol. 45, p. 2865 - 2877
参考文献
Jankowski,K.; Berse,C.
Canadian Journal of Chemistry, 1967 , vol. 45, p. 2865 - 2877
反应条件
1,4-dioxane; ammonia; water T=120°C;
参考文献
Jankowski,K.; Berse,C.
Canadian Journal of Chemistry, 1967 , vol. 45, p. 2865 - 2877
参考文献
Jankowski,K.; Berse,C.
Canadian Journal of Chemistry, 1967 , vol. 45, p. 2865 - 2877