反式-1,2-二苯乙烯氧化物合成路线 (共 213 条)
反应条件
Bacillus megaterium ECU1001 cell-free extract in potassium phosphate buffer; dimethyl sulfoxide T=30°C; pH=7; 0.166667 h; Resolution of racemateEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Zhao, Jing; Chu, Yan-Yan; Li, Ai-Tao; Ju, Xin; Kong, Xu-Dong; Pan, Jiang; Tang, Yun; Xu, Jian-He
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 9 p. 1510 - 1518
反应条件
PTAB; antimony(III)tribromide in dimethyl sulfoxide T=20°C; 40 h; Product distribution; Further Variations:ReagentsSolventsreaction times, reagent ratios;
参考文献
Sayama, Shinsei
Tetrahedron Letters, 2006 , vol. 47, # 24 p. 4001 - 4005
反应条件
bis-[(trifluoroacetoxy)iodo]benzene in dichloromethane 24 h; Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 46, p. 5231 - 5233
反应条件
Bacillus megaterium ECU1001 cell-free extract in potassium phosphate buffer; dimethyl sulfoxide T=30°C; pH=7; 0.166667 h; Resolution of racemateEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Zhao, Jing; Chu, Yan-Yan; Li, Ai-Tao; Ju, Xin; Kong, Xu-Dong; Pan, Jiang; Tang, Yun; Xu, Jian-He
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 9 p. 1510 - 1518
反应条件
PTAB; antimony(III)tribromide in dimethyl sulfoxide T=20°C; 40 h; Product distribution; Further Variations:ReagentsSolventsreaction times, reagent ratios;
参考文献
Sayama, Shinsei
Tetrahedron Letters, 2006 , vol. 47, # 24 p. 4001 - 4005
反应条件
bis-[(trifluoroacetoxy)iodo]benzene in dichloromethane 24 h; Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 46, p. 5231 - 5233
反应条件
Bacillus megaterium ECU1001 cell-free extract in potassium phosphate buffer; dimethyl sulfoxide T=30°C; pH=7; 0.166667 h; Resolution of racemateEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Zhao, Jing; Chu, Yan-Yan; Li, Ai-Tao; Ju, Xin; Kong, Xu-Dong; Pan, Jiang; Tang, Yun; Xu, Jian-He
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 9 p. 1510 - 1518
反应条件
PTAB; antimony(III)tribromide in dimethyl sulfoxide T=20°C; 40 h; Product distribution; Further Variations:ReagentsSolventsreaction times, reagent ratios;
参考文献
Sayama, Shinsei
Tetrahedron Letters, 2006 , vol. 47, # 24 p. 4001 - 4005
反应条件
1: MgBr2*Et2O; Amberlyst 15 / acetonitrile / 2 h / 0 °C 2: 95 percent / NaN3 / dimethylformamide / 12 h / 20 °C 3: 95 percent / H2 / 5 percent Pd/C / methanol / 12 h / 20 °C / atmospheric pressure View Scheme
参考文献
Lupattelli, Paolo; Bonini, Carlo; Caruso, Leonilde; Gambacorta, Augusto
Journal of Organic Chemistry, 2003 , vol. 68, # 8 p. 3360 - 3362
反应条件
1,4-dioxane; ammonia; water T=120°C;
参考文献
Jankowski,K.; Berse,C.
Canadian Journal of Chemistry, 1967 , vol. 45, p. 2865 - 2877