反式-1,2-二苯乙烯氧化物合成路线 （共 213 条）
反应条件
1.1: dioxane / 0.5 h / 20 °C 1.2: NaH / 1 h / 20 °C 2.1: 95 percent / Rh2(OAc)4; tetrahydrothiophene; BnEt3N(1+)*Cl(1-) / acetonitrile / 3 h / 40 °C View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 40, # 8 p. 1430 - 1433
反应条件
1: LiAlH4 / diethyl ether; tetrahydrofuran / 1.) 0 deg C, 18 h; 2.) 5 h, RT 2: diethoxytriphenylphosphorane / toluene / 18 h / 100 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 107, # 18 p. 5210 - 5219
反应条件
potassium tert-butylate in dimethyl sulfoxide; tert-butyl alcohol T=20°C; optical yield given as percent dediastereoselective reaction;
参考文献
Synlett, , # 19 art. no. W16611ST, p. 2823 - 2826
反应条件
[5,10,15,20-tetrakis(2,6-dichlorophenyl)porphinato]iron(III) chloride in dichloromethane; water; tert-butyl alcohol 4 h; Ambient temperature; Further byproducts given;
参考文献
Journal of the American Chemical Society, , vol. 113, # 7 p. 2747 - 2753
反应条件
dihydrogen peroxide; hexaaquairon(III) perchlorate; PYML-8 in methanol 0.5 h; Ambient temperatureother catalyst systems, other alkenes; Product distribution;
参考文献
Tetrahedron, , vol. 47, # 7 p. 1191 - 1204
反应条件
glyoxylic acid methylester methylhemiacetal; dihydrogen peroxide; [Mn2O3(1,4,7-trimethyl-1,4,7-triazacyclononane)2](PF6)2 in acetonitrile T=0°C;
参考文献
Tetrahedron Letters, , vol. 43, # 14 p. 2619 - 2622
反应条件
1: 2-Bromo-trans-stilbene Oxide With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 1.5 h; 2: methyl iodide in tetrahydrofuran; hexane
参考文献
Organic Letters, , vol. 6, # 23 p. 4191 - 4194
反应条件
in acetonitrile T=22°C; Corey-Chaikovsky reaction; Electrolysis;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 76, # 11 p. 2155 - 2165
反应条件
sodium hypochlorite; [NiCl2(py)4] in dichloromethane; water 5 h; Ambient temperature;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 64, # 10 p. 3185 - 3187
反应条件
sodium hypochlorite; [NiCl2(py)4] in dichloromethane; water 6 h; Ambient temperature;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 64, # 10 p. 3185 - 3187
