lithium hydroxide; triethylamine; Methanesulfonyl azide 1.) CH3CN, room temperature, 4 h, 2.) H2O, 5 h; Yield given. Multistep reaction;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '605283', constants.ctx, '0')">triethylamine</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '102391', constants.ctx, '0')">tetrahydrofuran</a> <br />&nbsp;1.) 0 deg C, 1 h, 2.) room temperature, 12 h;&nbsp;<br /> &nbsp;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '7366472', constants.ctx, '0')">zirconium oxide</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '9899153', constants.ctx, '0')">molybdenum</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '635760', constants.ctx, '0')">toluene</a> <br />T=109.85&deg;C;&nbsp;6&nbsp;h;&nbsp;<br /> &nbsp;

T=150&deg;C;&nbsp;&nbsp;unter Abdestillieren des gebildeten Aethanols;&nbsp;<br /> &nbsp;