N-(3-丁炔)邻苯二甲酰亚胺合成路线 （共 11 条）
反应条件
Mitsunobu conditions;
参考文献
Tiecco, Marcello; Testaferri, Lorenzo; Temperini, Andrea; Bagnoli, Luana; Marini, Francesca; Santi, Claudio; Terlizzi, Raffaella
European Journal of Organic Chemistry, 2004 , # 16 p. 3447 - 3458
反应条件
triphenylphosphine; diethylazodicarboxylate in tetrahydrofuran T=0 - 20°C; 5.41667 h;
参考文献
WO2004/96822 A2, ;
Page 260 ;
反应条件
sodium iodide in N,N-dimethyl-formamide T=100°C; 4.2 h;
参考文献
Hess, Wilfried; Burton, Jonathan W.
Chemistry - A European Journal, 2010 , vol. 16, # 41 p. 12303 - 12306
反应条件
tri-n-butylhexadecylphosphonium bromide in toluene T=40°C; 20 h;
参考文献
Jackson, W. Roy; Perlmutter, Patrick; Smallridge, Andrew J.
Australian Journal of Chemistry, 1988 , vol. 41, # 8 p. 1201 - 1208
参考文献
Tetrahedron Letters, , vol. 29, # 16 p. 1983 - 1984
反应条件
indium trifluoromethanesulfonate; water; toluene-4-sulfonic acid in 1,2-dichloro-ethane 5.8 h; Sealed tubeReflux; regioselective reaction;
参考文献
Gao, Qi; Li, Shenyan; Pan, Yingming; Xu, Yanli; Wang, Hengshan
Tetrahedron, 2013 , vol. 69, # 19 p. 3775 - 3781
反应条件
1: With hydrazine hydrate in ethanol T=20°C; 72 h; 2: With hydrogenchloride; water in ethanol 15 h;
参考文献
Hess, Wilfried; Burton, Jonathan W.
Chemistry - A European Journal, 2010 , vol. 16, # 41 p. 12303 - 12306
反应条件
1: With hydrazine hydrate in ethanol T=20°C; 72 h; 2: With hydrogenchloride; water in ethanol 15 h;
参考文献
Hess, Wilfried; Burton, Jonathan W.
Chemistry - A European Journal, 2010 , vol. 16, # 41 p. 12303 - 12306
反应条件
1: With hydrazine hydrate 1 h; Inert atmosphereReflux; 2: With hydrogenchloride in water Inert atmosphere;
参考文献
Karibe, Yusuke; Kusama, Hiroyuki; Iwasawa, Nobuharu
Angewandte Chemie - International Edition, 2012 , vol. 51, # 25 p. 6214 - 6218
反应条件
piperidine in DMF (N,N-dimethyl-formamide)
T=32 - 100°C;
参考文献
Wyeth
Patent: US2005/49296 A1, 2005 ;
Location in patent: Page/Page column 7 ;
