Boc-L-烯丙基甘氨酸二环己胺盐合成路线 （共 4 条）
反应条件
sodium hydroxide in diethyl ether; water 2 h;
参考文献
Allen, Norris E.; Boyd, Donald B.; Campbell, Jack B.; Deeter, Jack B.; Elzey, Thomas K.; et al.
Tetrahedron, 1989 , vol. 45, # 7 p. 1905 - 1928
反应条件
in N,N-dimethyl-formamide 72 h; Ambient temperature; Yield given;
参考文献
Allen, Norris E.; Boyd, Donald B.; Campbell, Jack B.; Deeter, Jack B.; Elzey, Thomas K.; et al.
Tetrahedron, 1989 , vol. 45, # 7 p. 1905 - 1928
反应条件
hydrogenchloride in water T=0°C;
参考文献
Takaya, Hikaru; Iwaya, Takashi; Ogata, Kazuki; Isozaki, Katsuhiro; Yokoi, Tomoya; Yoshida, Ryota; Yasuda, Nobuhiro; Seike, Hirofumi; Takenaka, Toshio; Nakamura, Masaharu
Synlett, 2013 , vol. 24, # 15 art. no. ST-2013-U0474-L, p. 1910 - 1914
反应条件
1: hydrogenchloride / ethyl acetate; water / pH 2.0
2: toluene; hexane; methanol / 2 h
View Scheme
参考文献
Takaya, Hikaru; Iwaya, Takashi; Ogata, Kazuki; Isozaki, Katsuhiro; Yokoi, Tomoya; Yoshida, Ryota; Yasuda, Nobuhiro; Seike, Hirofumi; Takenaka, Toshio; Nakamura, Masaharu
Synlett, 2013 , vol. 24, # 15 art. no. ST-2013-U0474-L, p. 1910 - 1914
