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63148-62-9
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
首页
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14399-53-2
合成路线
（共 27 条）
14399-53-2
+
107-18-6
烯丙醇
→
反应条件
反应条件
暂无反应条件数据
参考文献
Charette, Andre B.; Brochu, Christian
Journal of the American Chemical Society, 1995 , vol. 117, # 45 p. 11367 - 11368
2039-82-9
4-溴苯乙烯
+
14399-53-2
→
反应条件
1124-14-7
4-溴环丙基苯
反应条件
1: Zn(CH2I)2 With ethylene glycol dimethyl ether; trichloroacetic acid in hexane; dichloromethane T=-15°C; Simmons-Smith Cyclopropanation; 1 h; Schlenk techniqueInert atmosphere; 2: 1-bromo-4-ethenylbenzene in hexane; dichloromethane T=-15 - 25°C; Simmons-Smith Cyclopropanation; 18 h; Schlenk techniqueInert atmosphere;
参考文献
Cheng, Donghao; Huang, Deshun; Shi, Yian
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 34 p. 5588 - 5591
530-48-3
1,1-二苯乙烯
+
14399-53-2
→
反应条件
3282-18-6
(1-苯基环丙基)苯
反应条件
1: Zn(CH2I)2 With ethylene glycol dimethyl ether; trichloroacetic acid in hexane; dichloromethane T=-15°C; Simmons-Smith Cyclopropanation; 1 h; Schlenk techniqueInert atmosphere; 2: 1,1-di(phenyl)ethylene in hexane; dichloromethane T=-15 - 25°C; Simmons-Smith Cyclopropanation; 18 h; Schlenk techniqueInert atmosphere;
参考文献
Cheng, Donghao; Huang, Deshun; Shi, Yian
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 34 p. 5588 - 5591
14399-53-2
+
148017-75-8
→
反应条件
2437-56-1
1-十三烯
反应条件
1: dodecyl p-tolyl sulfoxide With lithium diisopropyl amide in tetrahydrofuran T=-70 - -40°C; 2: With copper(I) bromide in tetrahydrofuran T=-40 - 20°C; 0.5 h; 3: Zn(CH2I)2 in tetrahydrofuran T=20°C; 1 h;
参考文献
Abramovitch, Adi; Marek, Ilan
European Journal of Organic Chemistry, 2008 , # 29 p. 4924 - 4931
3220-49-3
+
14399-53-2
→
反应条件
2327-99-3
反应条件
1: copper phenyl; 1-ethynesulfinyl-4-methyl-benzene in tetrahydrofuran T=-70°C; 0.5 h; 2: Zn(CH2I)2 in tetrahydrofuran T=20°C; 0.0833333 h;
参考文献
Varghese, Jos P.; Zouev, Irena; Aufauvre, Lionel; Knochel, Paul; Marek, Ilan
European Journal of Organic Chemistry, 2002 , # 24 p. 4151 - 4158
14399-53-2
+
98-83-9
α-甲基苯乙烯
→
反应条件
2214-14-4
反应条件
1: Zn(CH2I)2 With ethylene glycol dimethyl ether; trichloroacetic acid in hexane; dichloromethane T=-15°C; Simmons-Smith Cyclopropanation; 1 h; Schlenk techniqueInert atmosphere; 2: isopropenylbenzene in hexane; dichloromethane T=-15 - 25°C; Simmons-Smith Cyclopropanation; 18 h; Schlenk techniqueInert atmosphere;
参考文献
Cheng, Donghao; Huang, Deshun; Shi, Yian
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 34 p. 5588 - 5591
14399-53-2
+
667447-32-7
→
反应条件
20826-80-6
己-1-烯-2-基苯
反应条件
1: 1-methyl-4-[(1-phenylpentyl)sulfinyl]benzene With lithium diisopropyl amide in tetrahydrofuran T=-70 - -40°C; 2: With n-butyllithium in tetrahydrofuran T=-70°C; 0.166667 h; 3: Zn(CH2I)2 in tetrahydrofuran T=-70 - 20°C;
参考文献
Abramovitch, Adi; Marek, Ilan
European Journal of Organic Chemistry, 2008 , # 29 p. 4924 - 4931
768-49-0
2-甲基-1-苯基丙烯
+
14399-53-2
→
反应条件
7653-94-3
1-苯基-2,2-二甲基环丙烷
反应条件
1: Zn(CH2I)2 With ethylene glycol dimethyl ether; trichloroacetic acid in hexane; dichloromethane T=-15°C; Simmons-Smith Cyclopropanation; 1 h; Schlenk techniqueInert atmosphere; 2: 2-methyl-1-phenyl-1-propene in hexane; dichloromethane T=-15 - 25°C; Simmons-Smith Cyclopropanation; 18 h; Schlenk techniqueInert atmosphere;
参考文献
Cheng, Donghao; Huang, Deshun; Shi, Yian
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 34 p. 5588 - 5591
75553-23-0
+
14399-53-2
→
反应条件
662143-14-8
反应条件
titanium tetrachloride in dichloromethane T=-20°C;
参考文献
Charette, Andre B.; Brochu, Christian
Journal of the American Chemical Society, 1995 , vol. 117, # 45 p. 11367 - 11368
2177-47-1
+
14399-53-2
→
反应条件
78926-56-4
反应条件
1: Zn(CH2I)2 With ethylene glycol dimethyl ether; trichloroacetic acid in hexane; dichloromethane T=-15°C; Simmons-Smith Cyclopropanation; 1 h; Schlenk techniqueInert atmosphere; 2: 2-methyl-indene in hexane; dichloromethane T=-15 - 25°C; Simmons-Smith Cyclopropanation; 20 h; Schlenk techniqueInert atmosphere;
参考文献
Cheng, Donghao; Huang, Deshun; Shi, Yian
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 34 p. 5588 - 5591
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