2,2,4-三甲基-1,3-戊二醇合成路线 (共 62 条)
反应条件
1: With carbon monoxide; hydrogen; triphenylphosphine; [rhodium(I)(carbonyl)2(acetylacetonate)]; L-proline in N,N-dimethyl-formamide T=5°C; P=22502.3 Torr; 48 h; 2: With sodium tetrahydroborate in methanol; N,N-dimethyl-formamide T=0°C; 0.666667 h; Further stages.;
参考文献
Abillard, Olivier; Breit, Bernhard
Advanced Synthesis and Catalysis, 2007 , vol. 349, # 11-12 p. 1891 - 1895
反应条件
nickel in sodium hydroxide T=20°C; Electrochemical reaction;
参考文献
Shchelkunov; Do; Bekenova
Russian Journal of Organic Chemistry, 2003 , vol. 39, # 5 p. 735 - 735
参考文献
Eastman Chemical Company
Patent: US5990321 A1, 1999 ;
反应条件
water; calcium carbonate T=150°C; P=40452.9 Torr;
反应条件
water; nickel T=50 - 85°C; Hydrogenation;
参考文献
DE939869 , ;
US2700685 , ;
反应条件
sodium amalgam; ethanol; sulfuric acid
参考文献
Bulletin de la Societe Chimique de France, , vol. <3>13, p. 1049
Monatshefte fuer Chemie, , vol. 17, p. 673
Monatshefte fuer Chemie, , vol. 17, p. 643
反应条件
potassium hydroxide zuletzt bei Siedetemperatur;
参考文献
Journal of the American Chemical Society, , vol. 70, p. 2593
反应条件
sodium hydroxide in water T=60°C; 4 h; Concentration; Overall yield = 63.6 percentChromat.;
参考文献
Chemical Papers, , vol. 68, # 3 p. 422 - 426
反应条件
sodium hydroxide in methanol
参考文献
Justus Liebigs Annalen der Chemie, , vol. 756, p. 162 - 169
反应条件
1: With sodium hydroxide T=60°C; 4 h; 2: With hydrogenchloride Concentration; Overall yield = 85.4 percentChromat.;
参考文献
Chemical Papers, , vol. 68, # 3 p. 422 - 426